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Beilstein J. Org. Chem. 2005, 1, No. 13, doi:10.1186/1860-5397-1-13
Graphical Abstract
Scheme 1: Reagents: i N3CH2C(O)F, AlMe3
Scheme 2: Reagents: i KF, DMF, 73%; ii NaOH, EtOH then aqHCl, 44%; iii (CO)2Cl2, 90%.
Scheme 3: Reagents: i iPr2EtN, Yb(OTf)3, 9, DCM, 92%; ii I2, THF/ H2O, Na2S2O3, 82%.
Scheme 4: Reagents i. I2, THF/H2O.
Scheme 5: Reagents: (a) I2, THF/H2O, Na2S2O3.
Scheme 6: Reagents: i iPr2EtN, Yb(OTf)3, 9 or PhCHFCOCl, DCM, 92%.
Scheme 7: Reagents: i. LiAlH4, THF, 99%; ii. HCl-Et2O.
Figure 1: ORTEP drawing of (2S, 2'S)-28 showing two crystallographically independent molecules within the uni...
Scheme 8: Reagents: (a) I2, THF/H2O, Na2S2O3.